BRITISH STANDARD

BS EN
14398-3:2003

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Incorporating
Amendment No.1

Cryogenic vessels —
Large transportable
non-vacuum insulated
vessels —
Part 3: Operational requirements

The European Standard EN 14398-3:2003, with the incorporation of
amendment A1:2005, has the status of a British Standard

ICS 23.020.40

12&23<,1*:,7+287%6,3(50,66,21(;&(37$63(50,77('%<&23<5,*+7/$:


BS EN 14398-3:2003

National foreword

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

This British Standard is the official English language version of

EN 14398-3:2003, including amendment A1:2005.
The start and finish of text introduced or altered by CEN amendment is
indicated in the text by tags !".Tags indicating changes to CEN text carry
the number of the CEN amendment. For example, text altered by CEN
amendment A1 is indicated by !".
The UK participation in its preparation was entrusted to Technical Committee
PVE/18, Cryogenic vessels which has the responsibility to:
—

aid enquirers to understand the text;

—

present to the responsible international/European committee any
enquiries on the interpretation, or proposals for change, and keep
UK interests informed;

—

monitor related international and European developments and
promulgate them in the UK.

A list of organizations represented on this committee can be obtained on
request to its secretary.
Cross-references
The British Standards which implement international or European
publications referred to in this document may be found in the BSI Catalogue
under the section entitled “International Standards Correspondence Index”, or
by using the “Search” facility of the BSI Electronic Catalogue or of British
Standards Online.

This publication does not purport to include all the necessary provisions of a
contract. Users are responsible for its correct application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.

This British Standard was
published under the authority
of the Standards Policy and
Strategy Committee
on 4 September 2003

Summary of pages
This document comprises a front cover, an inside front cover, the EN title page,
pages 2 to 18, an inside back cover and a back cover.
The BSI copyright notice displayed in this document indicates when the
document was last issued.

Amendments issued since publication

© BSI 7 March 2006

ISBN 0 580 42565 7

Amd. No.

Date

Comments

15917


March 2006

See national foreword


EN 14398-3

EUROPEAN STANDARD

August 2003

NORME EUROPÉENNE

+A1

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

EUROPÄISCHE NORM

July 2005

ICS 23.020.40

English version

Cryogenic vessels - Large transportable non-vacuum insulated
vessels - Part 3: Operational requirements
(includes amendment A1:2005)
Récipients cryogéniques - Grands récipients transportables

non isolés sous vide - Partie 3: Exigences de service
(inclut l'amendement A1:2005)

Kryo-Behälter - Große ortsbewegliche, nicht vakuumisolierte Behälter - Teil 3: Betriebsanforderungen
(enthält Änderungen A1:2005)

This European Standard was approved by CEN on 10 July 2003; amendment A1:2005 was approved by CEN on 17 June 2005.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and United
Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: rue de Stassart, 36

© 2003 CEN

All rights of exploitation in any form and by any means reserved
worldwide for CEN national Members.

B-1050 Brussels


Ref. No. EN 14398-3:2003+A1:2005 E


EN 14398-3:2003 (E)

Contents
Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Page
Foreword......................................................................................................................................................................3
Introduction .................................................................................................................................................................4
1

Scope ..............................................................................................................................................................5

2

Normative references ....................................................................................................................................5

3

Terms and definitions....................................................................................................................................5

4
4.1
4.2
4.3

Preliminaries before putting into service ....................................................................................................6
General............................................................................................................................................................6

Marking and placarding.................................................................................................................................6
Handover documents ....................................................................................................................................6

5

Personnel training .........................................................................................................................................6

6
6.1
6.2

General safety requirements ........................................................................................................................6
General............................................................................................................................................................6
Safety considerations....................................................................................................................................7

7

Putting into service........................................................................................................................................7

8

Location ..........................................................................................................................................................8

9

Transport within the location........................................................................................................................8

10
10.1
10.2

10.3

Filling...............................................................................................................................................................9
Prefill checks ..................................................................................................................................................9
Preparations ...................................................................................................................................................9
After fill check ..............................................................................................................................................10

11

Product withdrawal......................................................................................................................................10

12

Change of service ........................................................................................................................................10

13

Taking out of service ...................................................................................................................................11

14

Maintenance and repair...............................................................................................................................11

15

Periodic inspection ......................................................................................................................................12

16
16.1
16.1.1

16.1.2
16.2
16.3
16.4
16.5
16.6
16.7
16.8

Additional requirements for flammable gases..........................................................................................12
General safety requirements (see also clause 6 ) ......................................................................................12
General..........................................................................................................................................................12
Electrical equipment and installation/earthing .........................................................................................13
Putting into service (see also clause 7) ......................................................................................................13
Location (see also clause 8).........................................................................................................................13
Transport within the location (see also clause 9) ......................................................................................13
Filling (see also clause 10) ...........................................................................................................................13
Change of service (see also clause 12).......................................................................................................14
Taking out of service (see also clause 13)..................................................................................................14
Maintenance and repair (see also clause 14) .............................................................................................14

17

Emergency equipment/procedures............................................................................................................14

Annex A (informative).................................................................................................................................................15
Example of an emergency procedure .....................................................................................................................15
Annex B (informative).................................................................................................................................................16
Qualification of existing national large transportable cryogenic vessels for use in the European Union......16
B.1

Scope ............................................................................................................................................................16
B.2
Definitions and symbols .............................................................................................................................16
B.3
General requirement....................................................................................................................................16
B.4
Markings .......................................................................................................................................................17
B.5
Inspection report..........................................................................................................................................17
Bibliography ..............................................................................................................................................................18
2


Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

EN 14398-3:2003 (E)

Foreword
This document (EN 14398-3:2003) has been prepared by Technical Committee CEN/TC 268 “Cryogenic vessels”,
the secretariat of which is held by AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an identical text or
by endorsement, at the latest by February 2004, and conflicting national standards shall be withdrawn at the latest
by February 2004.
This document has been prepared under a mandate given to CEN by the European Commission and the European
Free Trade Association, and supports the objectives of the framework Directives on Transport of Dangerous
Goods.
This document has been prepared under a mandate given to CEN by the European Commission and the European
Free Trade Association, and supports the objectives of the framework Directives on Transport of Dangerous
Goods.
This European Standard has been submitted for reference into the RID and/or in the technical annexes of the ADR.

Therefore in this context the standards listed in the normative references and covering basic requirements of the
RID/ADR not addressed within the present standard are normative only when the standards themselves are
referred to in the RID and/or in the technical annexes of the ADR.
EN 14398 consists of the following parts under the general title, Cryogenic vessels – Large transportable non
vacuum insulated vessels :








Part 1 : Fundamental requirements;
Part 2 : Design, fabrication, inspection and testing;
Part 3 : Operational requirements.

The annexes A and B are informative.
This document includes a Bibliography.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal,
Slovakia, Spain, Sweden, Switzerland and the United Kingdom.

Foreword to amendment A1
This European Standard (EN 14398-3:2003/A1:2005) has been prepared by Technical Committee CEN/TC 268
“Cryogenic vessels”, the secretariat of which is held by AFNOR.
This Amendment to the European Standard EN 14398-3:2003 shall be given the status of a national standard,
either by publication of an identical text or by endorsement, at the latest by January 2006, and conflicting national
standards shall be withdrawn at the latest by January 2006.
This European Standard has been prepared under a mandate given to CEN by the European Commission and the
European Free Trade Association, and supports essential requirements of EU Directive(s).
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries

are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands,
Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

3


Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

EN 14398-3:2003 (E)

Introduction
Elements of this standard support the requirements of the framework Directives on Transport of Dangerous Goods
and other international, national or local requirements.
Large transportable cryogenic vessels are often partly equipped by the manufacturer, but can be installed or reinstalled by another party, such as the operator user or owner. For this reason some of the scope of this European
Standard, which includes putting into service, inspection, filling, maintenance and emergency procedure overlaps
with some of the Parts 1 and 2 of EN 14398.
Operational requirements for the usage of these vessels on public road, rail, sea and air are not covered in this
standard, but are defined in other international, national or local requirements.

4


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

1

Scope


1.1 This European Standard specifies operational requirements for large transportable non vacuum insulated
cryogenic vessels of more than 1000 l volume.
1.2

2

This European Standard applies to vessels designed for cryogenic fluids specified in EN 14398-1.

Normative references

This European Standard incorporates by dated or undated reference, provisions from other publications. These
normative references are cited at the appropriate places in the text, and the publications are listed hereafter. For
dated references, subsequent amendments to or revisions of any of these publications apply to this European
Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the
publication referred to applies (including amendments).
EN 12300, Cryogenic vessels - Cleanliness for cryogenic service.
EN 14398-1:2003, Cryogenic vessels – Large Transportable non-vacuum insulated vessels – Part 1: Fundamental
requirements.

3

Terms and definitions

For the purposes of this European Standard, the terms and definitions given in EN 14398-1:2003 and the following
apply.
3.1
putting into service
operation by which a vessel is prepared to be used. It applies to either a new vessel being used for the first time or
an existing vessel being returned to service

3.2
filling
operation by which a transportable vessel undergoes a prefill check, filling with a cryogenic fluid and an after fill
check
3.3
withdrawal
process by which product is taken from a vessel to the connected supply system
3.4
outdoor location
location outside of any building or structure and not enclosed by more than two walls
3.5
underground location
area or room whose ground or floor is on all sides sufficiently lower than the adjacent ground surfaces
3.6
vessel
vessel means large transportable cryogenic vessel as defined in EN 14398-1

5


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

4

Preliminaries before putting into service

4.1 General
Before putting into service, verification shall take place to ensure that the vessel is suitable for the intended service

and that the marking, placarding and handover documents are complete.

4.2 Marking and placarding
Marking and placarding shall be in accordance with the relevant transport regulations, see also EN 14398-1.

4.3 Handover documents
In addition to the manufacturer’s documentation, where necessary the cryogenic vessel shall be accompanied by
vessel specific documents and instructions for all items supplied covering:








the operation;
the auxiliary equipment;
the inspection records.

These documents shall be retained by the owner of the vessel.
The user shall have appropriate operating instructions available. Such instructions may be attached to the vessel in
a permanent manner, or carried by or available to the operator.

5

Personnel training

Only persons trained for the specific task shall be allowed to put into service, fill, handle, operate or maintain the
vessel.
The training programme shall include:















normal procedures;
product and hazard identification;
safe operating limits;
emergency procedures (see annex A);
physical and chemical properties of the vessel’s content and their effects on the human body;
personal protection.

Training shall be repeated as necessary to ensure that personnel remain competent. A record should be
maintained which details the training personnel have received.

6

General safety requirements

6.1 General
Before any operation the operator should ensure that all equipment is free from any obvious damage or defect
which can effect its safe operation.
Marking and placarding shall not be removed or defaced.
6


EN 14398-3:2003 (E)

Consideration should be given to the product properties and the use of appropriate personal protective equipment.


Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Parts under pressure shall be disconnected only if they have been previously depressurised.
When under pressure, leaking valves or connections may only be tightened using suitable tools and procedures.
Direct flame or direct intense heat shall never be used to raise the pressure or de-ice frozen valves.
All surfaces which may come in contact with the product shall be kept free from oil and grease. For cleanliness
requirements, see EN 12300.
Outlets, seals and transfer hoses shall be checked to be clean, dry and free from contaminants and visible defects
before connection.
Vessels and transfer hoses shall not be modified without proper authorisation.
Consideration, shall be given to actions in specific conditions, e. g. thunderstorm.
Normal operating valves should normally be opened and closed slowly.

6.2 Safety considerations
In all operations and training the following safety considerations shall be taken into account:











7

small amounts of cryogenic fluids will produce large volumes of vaporised gas. Spillage of cryogenic fluids can
result in an oxygen deficient atmosphere, or in the case of vaporising oxygen, in an oxygen enriched
atmosphere. Provision is to be made for appropriate measures to take account of this, e.g. ventilation;
due to the possibility of cold embrittlement, cryogenic fluids shall only be used in product systems with
components which are suitable for low temperatures;
vaporising cryogenic fluids produce gases that are heavier than air and can accumulate in lower areas (e.g.

pits, trenches);
because of their extremely low temperatures, cryogenic fluids will produce cold burns when coming into
contact with the skin. Cold burns can also be produced from contact with uninsulated equipment and pipe;
to avoid dry ice plugs, parts under pressure of carbon dioxide e.g. pipes, hoses, shall be disconnected only if
they have been previously carefully depressurized.

Putting into service

This operation shall follow a written procedure and the results of the steps involved should be recorded (e.g. in a
check list). Such lists should be retained by the operating company.
Vessels and accessories shall be visually checked for damage.
It shall be verified that:










vessel and accessories are appropriate for the intended service, comply with the flow-sheet and are
appropriately marked and labelled; all labels shall be clearly displayed and appropriate for the product;
appropriate relief device(s) with a set pressure not higher than the maximum allowable working pressure of the
vessel is (are) fitted. Any relief devices requiring approval shall be correctly stamped and matching certificates
shall be available;
all operational valves should be operable;
all required checks and tests have been carried out.
7


EN 14398-3:2003 (E)


Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

The vessel shall be purged with an appropriate gas at a temperature above 0 °C until the gas emerging from the
vessel is sufficiently dry and pure.
The vessel shall be cooled down according to the manufacturer’s recommendations. Steps shall be taken to avoid
uncontrolled pressure rise due to rapid liquid vaporisation. The cool down gas chosen shall take into account the
risk of solidification.
Measuring and controlling devices (e.g. level gauge, pressure gauge etc.,) shall be checked for correct operation or
setting.

8

Location

The requirements listed in this clause are valid for storage/parking as well as other activities such as filling,
withdrawal etc.:






















vessels shall be located in a suitable area such as in the open air or in a sufficiently ventilated enclosed area,
away from sources of heat (e.g. welding source, open fire etc.). Hot work shall be subject to appropriate safety

measures. The area shall be kept appropriately clean and suitable access shall be provided;
vessels should not be located underground. However, where this is unavoidable, relief valve outlet(s) should
be piped to a safe external venting point and the underground location shall have sufficient continuous
ventilation to deal with product releases arising from normal operation;
adequate ventilation shall be provided. In locations at, or above ground level, natural ventilation is generally
sufficient, provided that the room is large enough or that the outdoor area is not closely surrounded by walls. In
other circumstances, forced ventilation or other precautions shall be provided;
the floor of the designated transhipment area shall be level and strong enough to take the weight of the full
transport unit. The vessel shall be located at a sufficient distance from the normal paths used by people or
vehicles. Water accumulation in the vicinity of the vessel shall be avoided;
vessels and their components shall be protected against mechanical damage;
in case of emergency, adequate means of escape shall be provided. Emergency exits shall be kept clear at all
times;
all doors/gates should be preferably outward opening and wide enough to provide an easy access and exit
route for personnel;
a vessel should only be left parked unattended in a location such that operation of the vessel relief devices will
not constitute a hazard;
the operating area should be clearly marked with appropriate warning signs. These may be displayed on the
vessel ;
if vessels are indoors for extended periods (i.e. overnight or weekends) appropriate vent and relief valve
outlets should be piped to a safe place. The vent pipework shall be designed in such a way so as to prevent
rainwater accumulation, or blockage by airborne material;




operation by unauthorised persons should be prevented, e.g. locked valve cabinet.

9

Transport within the location


This section refers to the transport of filled vessels other than by public road, rail, water-ways, sea and air; these
activities are fully covered by specific regulations.
Before transport, the vessels shall be examined for signs of damage or leaks and valves shall be checked to
ensure that they are in the operating positions.
8


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Cryogenic vessels shall never be subjected to impacts or falls; these could damage the outer insulation and the
vessel itself. If any vessel is known to have been subjected to accidental impact or fall, this shall be reported to an
appropriate competent person before further use.
Vehicles used for transport shall have well ventilated cargo areas and shall have separate cargo and passenger
compartments. Vessels shall be transported in their correct transport position.

10 Filling
The following operations shall be carried out in accordance with a written procedure.

10.1 Prefill checks
Prior to filling the filler shall examine the condition of the vessel as given in table 1:
Table 1 — Prefill checks
Acceptance criteria for filling
Data plate

Present, legible and in accordance with EN 14398-1

Inspection date


Within required period

Product identification labels

Fitted and legible and correct product

Vessel, accessories

No obvious signs of damage, corrosion, contamination,
oil or grease; no unusual ice, indicating a defect

Manual valves

Operable

Safety relief devices

In place, free from ice or other visible obstructions

Filling couplings and transfer
hoses

All parts are free from damage, oil or grease:








Pressure gauge


correct connection fitted for product and cap-fitted if
required;
the maximum filling pressure is less than the
nominal pressure of the filling line;
the surface in contact with the product of couplings,
seals and transfer hoses are free from
contamination, oil, grease and water.

Positive pressure above triple point in vessel

The vessel shall not be filled if any of these acceptance criteria cannot be met. Prior to filling all non-compliances
shall be corrected.

10.2 Preparations
The vehicle carrying the vessel has to be immobilised by a appropriate device.
Depending on the type of the cryogenic vessel, it may be filled to capacity either by volume or by weight, taking into
account product density to the level the vessel is designed for. The necessary measuring equipment shall be in
good working order.
9


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

If there is no residual pressure in the vessel prior to filling it should be purged to remove possible contaminants. For
carbon dioxide vessels, only gaseous carbon dioxide should be used for purging.
If the vessel is warm, it should be cooled down according to the manufacturer’s recommendations. Carbon dioxide
vessels shall be pressurised with gaseous carbon dioxide before introducing liquefied gas.

The purity of the residual product in the vessel shall be analysed and recorded where required by specification.
Where the purity of the residual product is outside specification the vessel should be purged until it meets
specification.
The fill hose should be purged and cooled down.
Where it is necessary, the pressure shall be reduced by venting to facilitate safe filling. For carbon dioxide the
pressure shall not drop below 5 bar. Measures shall be taken to ensure that there is not unrequired back-flow
between the vessel and supply vessel.

10.3 After fill check
The vessel weight or level of contents and pressure shall be checked and, where necessary, the vessel should be
vented or drained to reach the values required by specification.
Where required by specification, the vessel contents shall be analysed and recorded.
The filler should check that all valves are in the correct position (open or closed) according to the instructions, that
no unusual cold spots have developed and that valves, piping and fittings are free from leaks.

11 Product withdrawal
The operator shall check that the vessel product and pressure are compatible with the supply system, that the
correct hose couplings are available and that the nominal pressure of the withdrawal line is greater than the
pressure developed by the withdrawal system e.g. pumping system.
Before connecting the vessel for withdrawal, the operator shall check that no unrequired backflow from the vessel
is possible and also that liquefied gas cannot become trapped without adequate pressure relief.
The vehicle carrying the vessel shall be immobilised by a appropriate device before connecting the hose.
Operating valves shall be returned for appropriate position for transport unless otherwise instructed.

12 Change of service
This operation shall follow a written procedure and the results of the steps involved should be recorded. Such
records should be retained by the operating company until the next change of service.
The procedure shall include the following:











10

check that the vessel, the pump and the accessories are designed for the intended service. Special attention
shall be given to this point if the vessel is intended for oxidising fluids;
depressurisation, emptying and disconnecting the vessel shall be performed in accordance with clause 13;
where it is suspected that the vessel may have been contaminated, it shall be cleaned by using a suitable
cleaning procedure. Special attention shall be given to this point if the vessel is intended for oxidising fluids;
the vessel placarding, couplings and transfer hoses shall be changed appropriate to the new product;


EN 14398-3:2003 (E)

If the vessel is intended for oxidising fluids, the following additional requirements shall be considered:

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI








the vessel and all piping and accessories shall be purged with inert gas until the outlet temperature is at least
close to ambient temperature. The purge gas inlet temperature shall never exceed the maximum operating
temperature of the vessel;
it shall be verified by suitable methods that the vessel and all piping and accessories are not contaminated by
hydrocarbons, see EN 12300;
before the vessel is filled with an oxidising fluid a competent person shall verify that the procedure has been

carried out correctly.

Thereafter, follow the procedure in clause 7 before filling the vessel.

13 Taking out of service
This operation shall follow a written procedure and the results of the steps involved should be recorded. If the
vessel is intended for further service, such records should be retained by the operating company.
The procedure shall include the following:










depressurisation and emptying of the vessel;
when depressurising the vessel, it shall be verified that the valve used for emptying is not obstructed;
the process shall be checked by monitoring pressure and level gauge/weight, if necessary;
due consideration should be given to the properties of the product involved (e.g. solidification of CO2 ).

If the vessel is intended to be taken into service again later, the following additional requirements shall be
considered:










the purging of the vessel and accessories with inert gas;
if the vessel may be used for oxidising fluids at a later time, the cleaning and hydrocarbon checking steps
outlined in clause 12 (necessary) should be applied when the vessel is taken out of service;

if the vessel is to be transported or stored/parked, protective caps should be fitted on all transfer couplings;
when in store, a slight positive pressure of dry inert gas should be maintained in the vessel and the vessel
shall be labelled accordingly.

If the vessel is to be scrapped, it shall be purged necessarily and labelled accordingly.

14 Maintenance and repair
Maintenance is required to ensure that the vessel remains in a safe, serviceable condition. The responsibility for its
maintenance and repair shall be established between the contracting parties (e.g. owner, user and filler). Following
maintenance, the vessel shall comply with the current approval documentation.
Maintenance generally comprises:










checking the condition of the vessel, accessories and the external supporting structure;
checking the operability of valves;
minor repairs, e.g. changing of seals;
cleaning external surfaces.
11


EN 14398-3:2003 (E)

Maintenance operations shall only be carried out by personnel trained for the task.

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI


Equipment shall not be removed until the directly connected system has been depressurised.
Modifications in design, materials and equipment or repairs shall be approved by a competent person and the
documentation updated accordingly (see also EN 14398-1).
Any leakage shall be rectified promptly and in a safe manner. Only suitable approved spare parts shall be used.
The suitability of the spare part shall be approved by a competent person.
Hot work (welding, soldering, heat treatment, etc.) shall be carried out to an equivalent procedure (fabrication,
qualification of personnel, testing, certification etc.) as during manufacture.
Vessels shall be internally clean, dry and free from particulate matter and vessels for oxidising fluids shall be free
from oil and grease (see also EN 12300).
!CO2-vessels shall be de-pressurised using a written procedure. Liquid carbon dioxide vessels that have lost pressure
shall be re-pressurised using a written procedure. The material properties of the vessel have to be considered."

15 Periodic inspection
The inspection shall be performed by a competent inspection body at intervals defined by the relevant regulation
for public road-, rail-, sea- or air- transport.
Following activities shall be performed:














equipment and safety device check. Safety valves shall be lift tested either in situ or off the vessel. Bursting
discs, where fitted, shall be checked for correct installation and rating. If satisfactory they do not require
replacement;
visual internal inspection after removing the insulation. Check for signs of damage or corrosion which may
effect the integrity. Visual internal inspection has to be carried out only if the vessel is assigned for by a
manhole;

visual external inspection. Check for signs of damage or corrosion which may effect the integrity. Check
content and legibility of data plate (see 4.1) and other markings;
leak test. A gas leak test using an inert gas or the working medium at 90 % of the maximum working pressure;
pressure test. The pressure test of the vessel shall be carried out with the test pressure according EN 14398-1;
all other equipment shall be checked for satisfactory functioning. Satisfactory inspection shall be confirmed;
(see EN 14398-1).

NOTE

For cryogenic flexible hoses see EN 12434.

16 Additional requirements for flammable gases
16.1 General safety requirements
16.1.1 General
Precautions shall be taken when approaching a leak as the product can ignite and produce a flame
(see also clause 6 )
Care should be taken in the choice of personnel clothing, to protect as much as practical against static charges and
flames. Anti-static footwear should be worn.
Fill/withdrawal connections shall be capped when not in use.
Spillage of flammable fluids can result in the risk of fire or explosion.

12


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

16.1.2 Electrical equipment and installation/earthing
All product system and ancillary electrical equipment shall be in accordance with the requirements of the

hazardous area classification in which it is being used.
All parts of the installation shall be bonded to ensure electrical continuity.
Major items of equipment (e.g. the vessel) shall be bonded directly to the earth point and shall not rely upon the
piping as a means to earth while filling, discharging and maintenance.
For transfilling processes, equalisation of the electrical potentials is necessary. (resistance < 10

)

In the classified area personnel shall not be permitted to carry sources of flame, or non-approved electrical
equipment. Consideration shall be given to equipment generating electromagnetic waves, e.g. mobile phones and
radio transmitters.

16.2 Putting into service (see also clause 7)
Prior to filling a vessel which is empty or depressurised e. g. such that air could have entered the tank, it shall be
purged with an inert gas. An appropriate procedure shall be followed and purging shall be continued until the gas
within the vessel can not result in a flammable mixture forming during filling.

16.3 Location (see also clause 8)
Vessels shall not be located underground.
Vessels shall not be filled or stored indoors.
Vessels which are connected to product withdrawal systems should be located outdoors. However, they may be
located indoors, providing the following requirements are met :










where forced ventilation is provided, appropriate classified equipment shall be used;
all relief valve outlets and vent valve outlets shall be piped to a safe external venting point. The fire resistance

of the materials in the vicinity of the vent discharge shall be considered;
gas detectors shall be fitted within the room, set to alarm when 25 % of the lower explosive limit is reached;
for vessels which are located indoors, the entire room in which the vessel is located shall be considered a
potentially hazardous area and be subject to individual assessment.

16.4 Transport within the location (see also clause 9)
Vessels should not be transported within the location unless fill connections are capped.
Vessels should not be transported in elevators or lifts.
Vessels should not be transported in enclosed compartments of vehicles.

16.5 Filling (see also clause 10)
If the vessel is empty or depressurised e.g. such that air could have entered the tank, follow the procedure given
under 16.2.
The filling procedure shall be controlled by the filler.
Before starting filling, the earthing conductor shall be connected and the filling hose(s) purged free of air and to the
required impurity level.
Filling shall only be undertaken outdoors.
13


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

16.6 Change of service (see also clause 12)
Vessels designed and used for flammable fluid service shall not be transferred to oxidising, or inert fluid service,
without appropriate purging, cleaning and design parameter verification by a competent person.
16.7 Taking out of service (see also clause 13)
The vessel shall be purged with inert gas until the flammable gas concentration in the inert gas is stabilised below
50 % of the lower explosive limit of the flammable gas in air.


16.8 Maintenance and repair (see also clause 14)
Where maintenance or repair work requires the vessel to be inerted, it shall be emptied using a safe procedure and
purged with inert gas until the concentration of flammable gas in the inert gas is stabilised below 50 % of the lower
explosive limit of the flammable gas in air.

17 Emergency equipment/procedures
Emergency procedures shall be made available to all appropriate personnel to cover fire or any other hazardous
events, e.g. spills, which may occur. It is advisable that emergency procedures are prepared in conjunction with the
emergency services and that local conditions are considered.
The procedure should consider:










the properties of the cryogenic fluids;
the quantities involved;
the local topography;
the design of the vessel.

The procedure should include:








listing of emergency equipment required;
nomination of back-up personnel/organisations for managing emergencies and procedures for contacting them

both during and outside working hours;
immediate self-help actions required (e.g. shut down, sounding alarms, evacuation from the area, summoning
help, etc.).

The procedures should be readily available to all personnel involved, regularly practised and periodically checked
to ensure that they are up to date.
As a minimum, fire fighting equipment should consist of one suitable fire extinguisher. If water is used to keep
equipment cool in the event of fire, it should not be sprayed near relief device vents, because of potential danger of
plugging vents with ice.
An example of an emergency procedure is given in annex A.

14


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Annex A
(informative)
Example of an emergency procedure
Table A.1
Product:

- non-flammable, non toxic, non oxidising cryogenic fluid.

Hazards:

– colourless, odourless liquid has a very low temperature and evaporates
readily.

– cold gas is heavier than air and spreads along the ground.
– cold gas is invisible but produces mist in contact with atmospheric
moisture.
– the gas will suffocate without warning.
– contact with liquid causes cold burns and severe damage to eyes.
– heating the vessel will cause a pressure rise with a risk of the vessel
bursting.

Personnel protection:

– safety goggles, protective clothing, shoes and gloves.

Equipment:

– oxygen analyser
– breathing apparatus

Fire fighting extinguisher (CO2 – water
dry chemical) equipment:
Emergency
alarm:

action

raise

the – evacuate all persons from the immediate danger area.
– notify fire brigade immediately (if necessary)
– isolate the area
– place warning signs

– keep upwind (outdoors)
– in case of leakage/spillage
– tighten up leaks if this can be done without risk.
– allow liquid to evaporate
– prevent liquid entering sewers, pits, trenches
– in case of fire: keep vessel cool by spraying with water, do not spray water
directly on valves or safety equipment, move the vessel to a safe location if
possible.

First aid:

– get medical assistance if symptoms of inhalation are noticed or there has
been product contact with skin or eyes.
– in case of contact with liquid, first thaw affected parts with tepid water, then
remove clothing carefully.

Important telephone numbers:
Fire brigade: ................................
Supervisor: ..................................
Hospital/Physician ......................
15


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Annex B
(informative)
Qualification of existing national large transportable cryogenic vessels for

use in the European Union

B.1 Scope
This annex defines those checks, inspections and tests which are performed in accordance with TPED in order to
qualify existing national large transportable cryogenic vessels to ensure their compliance with the ADR/RID
technical provisions for free movement and use within all Member States of the European Union.

B.2 Definitions and symbols



« » - Official stampmark required by the TPED to certify existing conforming to ADR for use through the European
Union.
“Inspection body” means a body according TPED

B.3 General requirement
B.3.1 The owner/user of the large transportable cryogenic vessels will indicate to the inspection body the types
and the number of transportable cryogenic vessels presented for qualification.
For each of the large transportable cryogenic vessel the following data are documented:























manufacturer;
serial number(s);
date of manufacture;
regulation to which the transportable cryogenic vessels were designed and manufactured;
working pressure;
test pressure;
diameter of the inner vessel;
minimum wall thickness of the inner vessel;
volume of the inner vessel;
product(s) for which the transportable cryogenic vessel is designed and manufactured.

The inspection body verifies that this list contains all the necessary information to clearly define the large
transportable cryogenic vessels.

16


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

B.3.2 The inspection body verifies that the wall thickness of the transportable cryogenic vessels is equal or
greater than the minimum wall thickness as calculated in accordance with EN 14398-2.
B.3.3 The inspection body verifies that manufacturing certificates, material certificates and test certificates are
available.
B.3.4

The inspection body performs the periodic inspection according to clause 15.


B.4 Markings



B.4.1 A transportable cryogenic vessel passing the periodic Inspection can be stamped with the mark « » if the
general requirements of clause B.3 have been fulfilled.
B.4.2 To avoid any confusion in the new countries of use the large transportable cryogenic vessels should be
marked:






either in accordance with EN 14398-1 ;
or in accordance with the authorised marking of the country of use and fulfilling ADR requirements.

B.5 Inspection report
The authorised inspection body prepares an inspection report for each or each type of large transportable
cryogenic vessel and confirm approval with the relevant requirements.

17


EN 14398-3:2003 (E)

Licensed Copy: sheffieldun sheffieldun, na, Tue Oct 31 02:01:48 GMT+00:00 2006, Uncontrolled Copy, (c) BSI

Bibliography
EN 12434, Cryogenic vessels – Cryogenic flexible hoses.
EN 14398-2, Cryogenic vessels – Large Transportable non vacuum insulated vessels – Part 2: Design, fabrication,
inspection and testing.


18